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Potentiometric Auto Titrator

Titration or potentiometer is a instrument used for quantitative chemical analysis.Titra smart is provided with a two point auto calibration and standardisation (zero offset). The potentiometric Autotitrator Titra smart is capable of displaying pH and mV of the sample with temperature compensation. The liquid path comprises Teflon material and glass tight burette which creates chemically inert system for any sensitive analysis.

The 21 CFR part 11 compliance has audit trail which logs all the activities with search facility, report generation and printing. There is also a Electronic Signature functionality in Titra smart. As a standard the potentiometric smart Titrator has a manual archive and data backup facility.

Call On: 9136909578

Sales Support: sales.mfd@labindia.com

Service Support: servicecoordinator@labindia.com

Standard Features of Potentiometric Auto Titrator Titra Smart

User interactive for ease of operation with protection against invalid entries.
Vortex stirrer for vigorous and homogenous stirring with specially designed glass propeller for total chemical inertness.
Quick interchangeable imported burette assemblies with intelligent recognition for its volume size. Burette factor for dispensing corrections is available for true end point calculations.
System recognises proper connectivity of other peripherals like Burette, Stirrer, Electrode etc. gives indication in case of improper connectivity.
Composite Differential Electrode Amplifier unit for Potentiometric and Voltametric / KF Titrations, having connectivity to various Electrodes. Temperature Sensor with 4-line measurement technique ensures correct temperature indication.
Large memory capacity for method storage with suitable scientific parameters having GLP compliance.
Standardised modes of titration, namely incremental, equilibrium of titration.
By selecting titration method, instrument prints the type of appropriate electrode.
During titration, the measured variable i.e. electrode potential (mV) or the pH value is shown on the display together with dispensed volume and number of End Points (EP) detected.
User selectable End Point (EP) evaluation up to 9 EP during the run, and calculation by first, last, largest, all or selected EP with display of results and printout.

21 CFR PART 11 COMPLIANCE

Audit Trail for all activities with search facility, report generation and printing.
200 User IDs with alphanumeric entries of user name, password and role based privileges selection.
Multi-level roles with password protection and complexity.
User authentication is per formed for each and every operation done.
Customizable PDF report file can be created through print.
USB Printing eliminates the need of serial port to connect with instrument. The user can take printout on any local or network printer as well.
Electronic signature functionality.
Manual Archive and Data Backup facility available.

Typical Specification

Principle

Volume determination by equivalence point, end point

mV range

±3200 mv

Accuracy

±0.1mV (±0.0016 pH)

Polarized Sensor Measurement range

0 to ±3200 mV I 0 to ±80 µA

Polarized Sensor Resolution

0.1 mVI 0.1 µA

Amplifier input impedance

> 10•12 ohms

Burette Resolution

1/20000 for 10 ml (i.e. 0.5 microlitre)

Burette Volume

5 ml, 1O ml & 25 ml available

Filling time

<20 sec

Keyboard

Qwerty Keyboard

Display

7" TOUCH SCREEN

Titration Head

(a) Manual stand with swivelling arm

Stirrer System

Microcontroller based variable speed, high torque vortex stirrer with digital indication. Magnetic Stirrer optional

Sensors

(1) Electrodes for Potentiometric titration - (pH, Ion, Redox, Argentometric, Non-Aqueous & complexometric).a) Any combination electrode.b) Differential Electrode System comprising sensing (Indicator) Electrode with BNC Connector and Reference Electrode with 4mm Banana Connector.
(2) Electrode for KF with BNC/TNC Connectors.
(3) Temperature sensor (PRT/PT100)

Calibration

3-point Calibration with user entered buffer values and standardisation with 7 pH buffer

End Point detection

a) Potentiometric

Cut-off criteria

a) Volume b) End point c) mV/pH.

Methods

1) Titrations - a) Acid base
b) Non-aqueous
c) Redox
d) Preciptiation
e) Complexometric
f) back titration
2) KF titration (Optional)

Results

a) Molarity
b) % Assay (wt)
c) % volume (ml)
d) ppm
e) mg/I
f) mg/g g) g/I
h) meq/I
I) moVkg
j) TAN and TBN for oil samples.

Method Storage

16 GB data storage capacity for 200 methods and results

REPORT FORMAT

1) Method parameter.
2) Titration analysis report.
3) Titration analysis condensed report.
4) Titration data table. 5) Titration graphic report -
i) µIv/s mV
ii) µIv/s First derivative
iii)µIv/s Second derivative
iv) µIv/s Time
6) Auto evaluation report
7) Statistics report
8) End Point Titration report
9) Calibration report

Input/Output peripheral interface

(a) Serial Port: 1Nos. - for Balance
(b) USB Connectivity for data backup, software upgradationand printer connectivity
(c) LaserJet printer connectivity through wireless LAN

Power

230 V AC ± 10%, 50 Hz.

Environmental Operating Conditions

a) Operation : a)Indoor
b) Temperature : Ambient to 45°C
c) Humidity: 5 to 90% non-condensing.

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